The Manual covers all the practical aspects of pharmaceutical chemistry as per the new syllabus prescribed by Pharmacy Council of India under ER 2020 for First Year Diploma in Pharmacy students. The experiments are divided into eight sections as per the new regulation.They cover limit tests, identification of anions and cations, volumetric analysis, assays, boiling and melting point determinations,synthesis,identification tests and qualitative analysis. This laboratory manual would serve as ready reckoner for teachers. It would save teachers' time of instructions and dictation. The students can directly write their observations and do calculations in the space provided on the left page.Thus,the students' time saved in writing the record can be utilized fruitfully for performing and understanding the practical as well as theoretical aspects of each experiment.